Spesifikasi Koehler KLA-1-TS Automatic Cloud and Pour Point Analyzer
Test Method
For Petroleum Products, cloud point and pour point of a petroleum product is an index of the lowest temperature of its utility for certain applications. The specimen is cooled at a specified rate and examined periodically. The highest temperature at which a cloud is first observed at the bottom of the test jar is recorded as the cloud point. The lowest temperature at which movement of the specimen is observed is recorded as the pour point.
Specifications
Conforms to the specifications of:
KLA-1-TS: ASTM D2500, D5771, D5772, D5773; DIN 51597; IP 219, IP 444, IP 445, IP 446; ISO 3015
KLA-2-TS: ASTM D97, D5853, D5950; IP 15, IP441; ISO 3016
KLA-3 TS: ASTM D97, D2500, D5771, D5772, D5773, D5853, D5950; DIN 51597; IP 15, IP 219, IP441, IP 444, IP 445, IP 446; ISO 3015, ISO 3016
Temperature Range:
One-Stage: +60°C to -45°C
Two-Stage: +60°C to -80°C
Resolution: 0.06°C
Accuracy: ±0.1°C
Repeatability / Reproducibility: as per standard test methods or better
Data Storage: < 60,000 analyses
Features
- Cloud Point Analyzer conforms to ASTM D2500, D5771, D5772, D5773 and related test methods
- Pour Point Analyzer conforms to ASTM D97, D5853, D5950 and related test methods
- Stand alone system with Integrated Touch Screen Panel PC
- Direct Cooling system eliminates the need for solvent cooling baths
- One-stage cooling system provides temperatures as low as -45°C and a two-stage cooling system down to -80°C
- Cloud Point measured by light pulsed emission on I.R spectrum through a coaxial fiber optic
- Pour Point measured by two PT100 detection probes placed on the surface of the product and a mechanical moving arm bringing the test jar to a horizontal position
Description
Cloud Point Detection–The cloud point detection system provides automated sample testing with the accuracy and repeatability in accordance with ASTM D2500, D5771, D5772, D5773 and related international test methods. The sophisticated dynamic measuring system emits a light pulse every 1°C from a coaxial fiber optic cable positioned above the test sample. The light pulse is then reflected off the silver bottom test jar to an optical sensor. The advanced software package analyzes the response of the light pulse. The initial appearance of crystallization is monitored by light scattering, signifying the cloud point of the sample. All clear and transparent oils are readily measured by the detection system, regardless of sample color.
Pour Point Detection–The pour point detection system provides automated sample testing with the accuracy and repeatability in accordance with ASTM D97, D5853, D5950 and related international test methods. The automated operation involves removing the sample from the cooling jacket at 3°C intervals and tilting it to a 90° angle as prescribed by the test method until no flow is observed. Contact of the cold sample with the two PT100 detection probes positioned just above the surface liquid level when the test jar is tilted identifies sample flow. The test jar is automatically returned to the cooling jacket and sampled again until no flow is detected for 5 seconds. The pour point result is then reported at 3°C higher than the temperature at which the sample ceased to flow in accordance with the test method.
Integrated Panel PC and Software Package–The Automated Cloud and Pour Point Analyzers are complete standalone systems featuring an integrated panel PC with an advanced software package. The 6.4” TFT/LCD touch screen display has a resolution of 640x480 with a 262K color scheme. All analytical parameters are graphed and displayed in real time as well as recorded in Microsoft® Excel compatible file format. The software monitors the operation and performance of all the analyzer components for proper data measurement, including the solenoid valves, cooling system, pressure sensors, and the Platinum resistance PT100 Class A temperature probe.
Cooling System–For various user applications, the automated cloud and pour point systems are available with either one-stage cooling for temperatures as low as -45°C or two-stage cooling for temperatures as low as -80°C. The direct cooling system features integrated gas CFC free motors compressors thus eliminating the need for a solvent cooling bath. The direct system is capable of rapid cooling, approaching -80°C bath temperatures in approximately 15 minutes, and utilizes less electricity than standard cooling systems. The rapid cooling feature combined with a consistent cooling profile system provides repeatable results with high test reproducibility.
Multiple Configuration System–These automated sample cooling and physical property measurement systems can be configured with one, two, three, four and six test positions with one of five possible analytical heads at each position: cloud point, pour point, cloud & pour point, cold filter plugging point and freezing point. Standard and customized multiple configuration systems are readily available
Electrical Requirements
115V ± 15% / 60Hz
220V ± 15% / 50 to 60Hz
Additional Accessories
- K60002-LT-1 Rotor Assembly for Long Tubes
- K61101 Centrifuge Tube, Long, 100mL, 8”, marked in mL (ASTM D91, D96, D893, D1796, D4007)
- K61106 Centrifuge Tube, Long, 100mL, 8”, marked in 200 parts (ASTM D96)
- K61110 Centrifuge Tube, Long, 100mL, 8”, marked in mL every 1mL above 10ml (ASTM D96, D4007)
- K61112 Centrifuge Tube, Long, 100mL, 8”, marked in 200 parts every 2 parts above 20 parts (ASTM D96)
- K61109 Centrifuge Tube, Cone-Shaped, 100mL with capillary tip capable of measuring 0.01 mL and readable by estimation to 0.005%
- (ASTM D2273, D2709) (K61153 cushion required for each tube)
- K61135 PTFE cushion for Long Tubes
- K61153 PTFE cushion for Long Tubes with capillary tip (Required for K61109 tubes)
- K60002-ST-1 Rotor Assembly for Short Tubes
- K61102 Centrifuge Tube, Short, 100mL, 6”, marked in 200 parts every 4 parts above 20mL (ASTM D96)
- K61105 Centrifuge Tube, Short, 100mL, 6”, marked in mL (ASTM D96)
- K61107 Centrifuge Tube, Short, 100mL, 6”, marked in mL every 2mL above 10mL (ASTM D96)
- K61108 Centrifuge Tube, Short, 100mL, 6”, marked in 200 parts (ASTM D96)
- K61146 PTFE cushion for Short Tubes
- K60002-PT-1 Rotor Assembly for Pear Tubes
- K61104 Centrifuge Tube, Pear, 100mL, marked in mL
- K61152 Centrifuge Tube, Pear, 100mL, with tube tip having graduations of 0.01mL over the range 0 to 0.2mL (ASTM D2709)
- K61111 Cork Stopper for Long, Short and Pear Tubes
- K60002-FT-1 Rotor Assembly for Finger Tubes
- K61141 Centrifuge Tube, Finger Tube (API 2542)
- K61136 Felt support for Finger Tube
- K61132 Cork Stopper for Finger Tube
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